N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

Base Information

Chemical Name:N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide
CAS No.:1621377-87-4
Molecular Formula:C₂₀H₁₅F₃N₄O₂
Molecular Weight:400.36
Hs Code.:

Synonyms:N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

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Chemical Property of N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

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Technology Process of N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

There total 4 articles about N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1621377-99-8
4-nitro-N-(4-(trifluoromethyl)phenyl)benzimidoyl chloride

: 100-63-0
phenylhydrazine

: 1621377-87-4
N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo500898e

Reference yield:

: 62-23-7
4-nitro-benzoic acid

: 1621377-87-4
N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: thionyl chloride / Inert atmosphere; Reflux

4: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With thionyl chloride; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jo500898e

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1621377-87-4
N'-phenyl-N-[4-(trifluoromethyl)phenyl]-4-nitrobenzenecarbohydrazonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: thionyl chloride / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo500898e