3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

Base Information

Chemical Name:3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol
CAS No.:1395093-67-0
Molecular Formula:C₂₇H₂₆N₂O
Molecular Weight:394.516
Hs Code.:

Synonyms:3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

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Chemical Property of 3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

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Technology Process of 3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

There total 12 articles about 3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1395093-64-7
3-(2,6-diisopropylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

: 1395093-67-0
3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 18h;

Reference yield:

: 191171-55-8
2-anilineboronic acid pinacol ester

: 1395093-67-0
3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 24 h / 60 °C / Reflux

3.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / 18 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon; platinum on carbon / ethanol / 12 h / 2585.81 Torr / Inert atmosphere

5.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; hydrogen; boron tribromide; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; platinum on carbon; In ethanol; dichloromethane; water; isopropyl alcohol; toluene;

Reference yield:

: 138642-47-4
2-bromo-5-methoxybenzonitrile

: 1395093-67-0
3-(2,6-diisopropylphenyl)imidazo[1,2-f]phenanthridin-11-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 24 h / 60 °C / Reflux

3.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / 18 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon; platinum on carbon / ethanol / 12 h / 2585.81 Torr / Inert atmosphere

5.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; hydrogen; boron tribromide; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium 10% on activated carbon; platinum on carbon; In ethanol; dichloromethane; water; isopropyl alcohol; toluene;