bis(acetoxy)iodylbenzene

Base Information

• Chemical Name: bis(acetoxy)iodylbenzene
• CAS No.: 16975-78-3
• Molecular Formula: C₁₀H₁₁IO₅
• Molecular Weight: 338.099

Synonyms:bis(acetoxy)iodylbenzene

Chemical Property of bis(acetoxy)iodylbenzene

Chemical Property:

Purity/Quality:

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Technology Process of bis(acetoxy)iodylbenzene

There total 2 articles about bis(acetoxy)iodylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

iodoxybenzene (696-33-3) + acetic anhydride (108-24-7) → bis(acetoxy)iodylbenzene (16975-78-3)

Guidance literature:

at 20 ℃; for 3h;

DOI:10.1002/anie.201909868

Reference yield:

iodoxybenzene (696-33-3) + acetic acid (64-19-7,77671-22-8) → bis(acetoxy)iodylbenzene (16975-78-3)

Guidance literature:

With acetic anhydride;

Reference yield: 91.0%

[2,2]bipyridinyl (366-18-7) + trimethylsilyl trifluoromethanesulfonate (27607-77-8) + bis(acetoxy)iodylbenzene (16975-78-3) → 2,2’-bipyridyl λ5-iodane bistriflate

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/S0040-4039(02)01192-9

upstream raw materials:

iodoxybenzene

acetic anhydride

acetic acid

Downstream raw materials:

iodosylbenzene

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