{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

Base Information

Chemical Name:{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone
CAS No.:891829-95-1
Molecular Formula:C₂₃H₃₂O₄Si
Molecular Weight:400.59
Hs Code.:

Synonyms:{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

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Technology Process of {2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

There total 3 articles about {2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 891829-94-0
[2-(2-hydroxy-ethyl)-6-methoxy-phenyl]-(3-methoxy-phenyl)-methanone

: 18162-48-6
tert-butyldimethylsilyl chloride

: 891829-95-1
{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ol060556c

Reference yield:

: 30404-50-3
8-methoxy-3,4-dihydroisocoumarin

: 891829-95-1
{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂; tetrahydrofuran / -78 - 20 °C

2: 100 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

With 1H-imidazole; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol060556c

Reference yield:

: 36282-40-3
(3-methoxyphenyl)magnesium bromide

: 891829-95-1
{2-[2-(tert-butyldimethylsilanyloxy)ethyl]-6-methoxyphenyl}-(3-methoxyphenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂; tetrahydrofuran / -78 - 20 °C

2: 100 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

With 1H-imidazole; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol060556c