dibromobis(α-benzyl oximato)ruthenium(III)

Base Information

Chemical Name:dibromobis(α-benzyl oximato)ruthenium(III)
CAS No.:75400-20-3
Molecular Formula:C₂₈H₂₁Br₂N₂O₄Ru
Molecular Weight:710.364
Hs Code.:

Synonyms:dibromobis(α-benzyl oximato)ruthenium(III)

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Chemical Property of dibromobis(α-benzyl oximato)ruthenium(III)

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Technology Process of dibromobis(α-benzyl oximato)ruthenium(III)

There total 1 articles about dibromobis(α-benzyl oximato)ruthenium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 574-15-2,574-16-3,14090-77-8,5351-34-8
benzilmonoxime

: 75400-20-3
dibromobis(α-benzyl oximato)ruthenium(III)

Guidance literature:: With LiBr; In ethanol; soln. RuCl3*3H2O and LiBr in abs. ethanol stirred for 10 min, α-benzyl oxime added, mixt. warmed to 50°C and stirred for 2 h, thancooled to 0°C; ppt. filtered and washed with water and ethanol, crystals dried in vacuo over P4O10 and recrystd. from dichloromethane-diethyl ether; elem. anal.;

Reference yield:

: 75400-20-3
dibromobis(α-benzyl oximato)ruthenium(III)

: 75400-22-5
(RuBr₂(C₆H₅C(O)C(NO)C₆H₅)2H)^(1-)

Guidance literature:: In acetonitrile; Electrochem. Process; dibromobis(α-benzyl oximato)ruthenium(III) coulometrically reduced in acetonitrile;

Reference yield:

: 75400-20-3
dibromobis(α-benzyl oximato)ruthenium(III)

: 7632-00-0
sodium nitrite

: 174094-73-6
RuC₂₈H₂₀N₃O₅Br

Guidance literature:: With HCl; In methanol; trituration (323 K, 2 h), extn. (CHCl3); soln. evapn. (red. pressure), pptn., washing (ether), redissoln. (methanol-water), soln. evapn., pptn., drying (vac.); IR monitoring at 1900 cm**-1, elem. anal.;