2-hydroxyethyl p-phenyl ether

Base Information

• Chemical Name: 2-hydroxyethyl p-phenyl ether
• CAS No.: 224784-42-3
• Molecular Formula: C₃₉H₄₈O₂
• Molecular Weight: 548.809

Synonyms:2-hydroxyethyl p-phenyl ether

Chemical Property of 2-hydroxyethyl p-phenyl ether

Chemical Property:

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Technology Process of 2-hydroxyethyl p-phenyl ether

There total 2 articles about 2-hydroxyethyl p-phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) → 2-hydroxyethyl p-phenyl ether (224784-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.46 g / K₂CO₃ / dimethylformamide / 18 h / 65 °C

2: aq. HCl, EtOH / 16 h / Heating

With hydrogenchloride; ethanol; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/ja984051w

Reference yield:

2-(2-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-tetrahydro-pyran → 2-hydroxyethyl p-phenyl ether (224784-42-3)

Guidance literature:

With hydrogenchloride; ethanol; for 16h; Yield given; Heating;

DOI:10.1021/ja984051w

Reference yield: 97.0%

methanesulfonyl chloride (124-63-0) + 2-hydroxyethyl p-phenyl ether (224784-42-3) → 2-methanesulfonylethyl p-phenyl ether (224784-43-4)

Guidance literature:

With triethylamine; In dichloromethane; at -2 ℃; for 3.5h;

DOI:10.1021/ja984051w

upstream raw materials:

4-[tris-(4-tert-butylphenyl)methyl]phenol

Downstream raw materials:

2-methanesulfonylethyl p-phenyl ether

2-bromoethyl p-phenyl ether

1-(2-azidoethoxy)-4-(tris(4-tert-butylphenyl)methyl)benzene

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