tricarbonylrhenium(η(5)-C5H4C6H4Br)

Base Information

Chemical Name:tricarbonylrhenium(η(5)-C5H4C6H4Br)
CAS No.:219967-89-2
Molecular Formula:C₁₄H₈BrO₃Re
Molecular Weight:490.327
Hs Code.:

Synonyms:tricarbonylrhenium(η(5)-C5H4C6H4Br)

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Chemical Property of tricarbonylrhenium(η(5)-C5H4C6H4Br)

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Technology Process of tricarbonylrhenium(η(5)-C5H4C6H4Br)

There total 1 articles about tricarbonylrhenium(η(5)-C5H4C6H4Br) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: 1192-27-4
5-diazo-1,3-cyclopentadiene

: 5467-74-3
4-Bromophenylboronic acid

: 2923-28-6
silver trifluoromethanesulfonate

: 219967-89-2
tricarbonylrhenium(η(5)-C5H4C6H4Br)

Guidance literature:: With triethylamine; In acetonitrile; byproducts: AgBr; treating soln. of Re-complex with 3 equivs. of AgOTf, filtration off of AgBr, addn. of slightly excess of diazocyclopentadiene, 2 equivs. of boronic acid and 4 equivs. of Et3N, heating to 80°C for 14 h; concn.; chromy.;
DOI:10.1021/om990128t