N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

Base Information

Chemical Name:N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide
CAS No.:1361413-95-7
Molecular Formula:C₂₅H₂₃N₃O₃S
Molecular Weight:445.542
Hs Code.:

Synonyms:N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

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Chemical Property of N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

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Technology Process of N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

There total 4 articles about N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17061-62-0
N,N-bis(p-methoxybenzyl)amine

: 1147550-11-5
ammonium thiocyanate

: 1711-11-1
3-cyanobenzoyl chloride

: 1361413-95-7
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

Guidance literature:: In acetone;
DOI:10.1016/j.bmc.2013.12.021

Reference yield:

: ammonium thiocyanate

: 17061-62-0
N,N-bis(p-methoxybenzyl)amine

: 1711-11-1
3-cyanobenzoyl chloride

: 1361413-95-7
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

Guidance literature:: ammonium thiocyanate; 3-cyanobenzoyl chloride; In acetone; at 0 ℃; for 1.5h;

N,N-bis(p-methoxybenzyl)amine; In acetone; at 0 ℃; for 0.5h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1361413-95-7
N-[(bis{[4-(methyloxy)phenyl]methyl}amino)carbonothioyl]-3-cyanobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 3 h / Reflux

1.2: 0 - 20 °C

2.1: acetone / 1.5 h / 0 °C

2.2: 0.5 h / 0 °C

In methanol; acetone;