O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Base Information

Chemical Name:O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine
CAS No.:250602-93-8
Molecular Formula:C₁₃H₂₃NO₂Si
Molecular Weight:253.417
Hs Code.:

Synonyms:O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Suppliers and Price of O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Chemical Property:

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Technology Process of O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

There total 6 articles about O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 250602-93-8
O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Guidance literature:

Reference yield:

: 250602-92-7
N-[4-(tert-butyldimethylsilyloxy)benzyloxy]phtalimide

: 250602-93-8
O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; ethanol; at 60 ℃; for 1h;
DOI:10.1248/cpb.51.138

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 250602-93-8
O-[[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]methyl]hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / tetrahydrofuran; methanol / 0.5 h / 0 °C

2: 43 percent / DEAD; PPh₃ / 18 h / 20 °C

3: hydrazine monohydrate / tetrahydrofuran; ethanol / 1 h / 60 °C

With sodium tetrahydroborate; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; 2: Mitsunobu reaction;
DOI:10.1248/cpb.51.138