N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Base Information

Chemical Name:N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide
CAS No.:1020166-38-4
Molecular Formula:C₁₉H₁₈N₄O₃S
Molecular Weight:382.443
Hs Code.:

Synonyms:N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

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Chemical Property of N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

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Technology Process of N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

There total 5 articles about N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: (E)-4-(2-(1-phenylethylidene)hydrazinyl)benzenesulfonamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1020166-38-4
N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Guidance literature:: N,N-dimethyl-formamide; With trichlorophosphate; at 20 ℃; Reflux;

(E)-4-(2-(1-phenylethylidene)hydrazinyl)benzenesulfonamide; at 70 - 80 ℃;
DOI:10.2174/1570180817999201001160414

Reference yield:

: 1135952-91-8
C₁₄H₁₅N₃O₂S

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1020166-38-4
N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Guidance literature:: C₁₄H₁₅N₃O₂S; N,N-dimethyl-formamide; With trichlorophosphate; at 55 - 60 ℃; for 5h;

With sodium hydrogencarbonate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.01.060

Reference yield:

: 98-86-2
acetophenone

: 1020166-38-4
N'-((4-(4-formyl-3-phenyl-1H-pyrazol-1-yl)phenyl)sulfonyl)-N,N-dimethylformimidamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / water

1.2: 1 h / Reflux

2.1: trichlorophosphate / 5 h / 55 - 60 °C

With sodium acetate; trichlorophosphate; In water;
DOI:10.1016/j.ejmech.2011.01.060