5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

Base Information

Chemical Name:5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole
CAS No.:331242-53-6
Molecular Formula:C₂₇H₃₇NO₅Si
Molecular Weight:483.68
Hs Code.:

Synonyms:5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

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Technology Process of 5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

There total 5 articles about 5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 173900-19-1
3-bromomethyl-5-[3-(tert-butyldiphenylsilyloxy)propyl]isoxazole

: 111-46-6
diethylene glycol

: 331242-53-6
5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1071/CH03295

Reference yield: 67.0%

: 331242-53-6
5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

Guidance literature:

Reference yield:

: 331242-52-5
3-(tert-butyldimethylsilyloxymethyl)-5-[3-(tert-butyldiphenylsilyloxy)propyl]isoxazole

: 331242-53-6
5-[3-(tert-butyldiphenylsilyloxy)propyl]-3-[2-(2-hydroxyethoxy)ethoxymethyl]isoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / aq. HCl / tetrahydrofuran

2: 75 percent / PPh₃; Br₂

3: 67 percent / NaH; Bu₄NI / tetrahydrofuran

With hydrogenchloride; bromine; tetra-(n-butyl)ammonium iodide; sodium hydride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1071/CH03295