ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

Base Information

Chemical Name:ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate
CAS No.:134420-77-2
Molecular Formula:C₂₃H₃₅NO₆
Molecular Weight:421.534
Hs Code.:

Synonyms:ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

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Chemical Property of ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

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Technology Process of ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

There total 3 articles about ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 134420-72-7
ethyl N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

: 134420-77-2
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

Guidance literature:: With potassium carbonate; In 1,4-dioxane; a) 0 deg C, 15 min, b) RT, 3 h;
DOI:10.1021/jm00112a032

Reference yield:

: 134420-70-5
3-amino-5-phenyl-pentanoic acid ethyl ester

: 134420-77-2
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / ethanol / Ambient temperature

2: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

With potassium carbonate; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00112a032

Reference yield:

: 140-88-5,9003-32-1
ethyl acrylate

: 134420-77-2
ethyl N-(tert-butyloxycarbonyl)-N-(2-carbethoxyethyl)-3-amino-5-phenylvalerate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / ethanol / Ambient temperature

2: 95 percent / 5percent aq. potassium carbonate / dioxane / a) 0 deg C, 15 min, b) RT, 3 h

With potassium carbonate; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00112a032