2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Base Information

Chemical Name:2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol
CAS No.:213970-38-8
Molecular Formula:C₂₀H₂₆O₆
Molecular Weight:362.423
Hs Code.:

Synonyms:2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

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Chemical Property of 2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

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Technology Process of 2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

There total 5 articles about 2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 213970-33-3
methyl 2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)propanoate

: 213970-38-8
2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.333333h; Ambient temperature;
DOI:10.3987/com-98-8149

Reference yield:

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 213970-38-8
2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / NaH / dimethylformamide / Ambient temperature

2: 96 percent / NaBH₄ / tetrahydrofuran; ethanol / 0.75 h / Ambient temperature

3: 70 percent / LiBr, 2,6-lutidine, methanesulfonic anhydride / tetrahydrofuran / 30 h / Ambient temperature

4: 42 percent / n-BuLi, isopropylcyclohexylamine, HMPA / tetrahydrofuran; hexane / 0.5 h / -78 °C

5: 79 percent / LiAlH₄ / diethyl ether / 0.33 h / Ambient temperature

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; N-cyclohexylisopropylamine; sodium hydride; lithium bromide; Methanesulfonic anhydride; In tetrahydrofuran; diethyl ether; ethanol; hexane; N,N-dimethyl-formamide;
DOI:10.3987/com-98-8149

Reference yield:

: 124555-63-1
4-methoxy-2-methoxymethoxy benzaldehyde

: 213970-38-8
2-(2,4-dimethoxyphenyl)-3-(4-methoxy-2-O-methoxymethylphenyl)-1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaBH₄ / tetrahydrofuran; ethanol / 0.75 h / Ambient temperature

2: 70 percent / LiBr, 2,6-lutidine, methanesulfonic anhydride / tetrahydrofuran / 30 h / Ambient temperature

3: 42 percent / n-BuLi, isopropylcyclohexylamine, HMPA / tetrahydrofuran; hexane / 0.5 h / -78 °C

4: 79 percent / LiAlH₄ / diethyl ether / 0.33 h / Ambient temperature

With 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; lithium aluminium tetrahydride; n-butyllithium; N-cyclohexylisopropylamine; lithium bromide; Methanesulfonic anhydride; In tetrahydrofuran; diethyl ether; ethanol; hexane;
DOI:10.3987/com-98-8149