(CH₃)3NGeH₂

Base Information

• Chemical Name: (CH₃)3NGeH₂
• CAS No.: 118983-02-1
• Molecular Formula: C₃H₁₁GeN
• Molecular Weight: 133.717
• Mol file: 118983-02-1.mol

Synonyms:(CH₃)3NGeH₂

Chemical Property of (CH₃)3NGeH₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (CH₃)3NGeH₂

There total 1 articles about (CH₃)3NGeH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromogermanate (13569-43-2) → (CH3)3NGeH2 (118983-02-1) + trimethyl ammonium bromide (2840-24-6)

Guidance literature:

With trimethylamine; In diethylene glycol; under N2 or in vac., allowed to react at -78 to 0°C; pptn. filtered off at 0°C, solid extd. (H2O), not isolated;

DOI:10.1016/S0020-1693(00)85155-5

Reference yield:

(CH3)3NGeH2 (118983-02-1) + trimethylgermane (1449-63-4) → germane (7782-65-2) + trigermane (14691-44-2) + tetragermane (14691-47-5) + (CH3)3Ge2H3

Guidance literature:

In diethylene glycol; under N2 or in vac., 10-30 fold excess of Me3GeH, stirred and warmed to 0°C (0.3-2 h) and 25°C (0.5-17 h);

DOI:10.1016/S0020-1693(00)85155-5

Reference yield:

(CH3)3NGeH2 (118983-02-1) + dimethylgermane (1449-64-5) → germane (7782-65-2) + trigermane (14691-44-2) + tetragermane (14691-47-5) + (CH3)2Ge2H4

Guidance literature:

In diethylene glycol; under N2 or in vac., 10-30 fold excess of Me2GeH2, stirred and warmed to 0°C (0.3-2 h) and 25°C (0.5-17 h);

DOI:10.1016/S0020-1693(00)85155-5

upstream raw materials:

bromogermanate

Downstream raw materials:

germane

trigermane

tetragermane

chlorogermane