2,2-dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione

Base Information

• Chemical Name: 2,2-dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione
• CAS No.: 133709-17-8
• Molecular Formula: C₂₂H₂₆O₄
• Molecular Weight: 354.446
• Mol file: 133709-17-8.mol

Synonyms:2,2-Dimethyl-5-(2-phenyltricyclo<3.3.1.1^3,7>decan-2-yl)-1,3-dioxane-4,6-dione

Chemical Property of 2,2-dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione

Chemical Property:

Purity/Quality:

2,2-Dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione

There total 1 articles about 2,2-dimethyl-5-(2-phenyl-2-adamantyl)-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,2-Dimethyl-5-(tricyclo<3.3.1.13,7>decanylidene)-1,3-dioxane-4,6-dione (51757-47-2) + phenylmagnesium bromide → 2-phenyladamantan-2-ol (29480-18-0) + 2,2-Dimethyl-5-(2-phenyltricyclo<3.3.1.13,7>decan-2-yl)-1,3-dioxane-4,6-dione (133709-17-8)

Guidance literature:

copper(I) bromide; In diethyl ether; 1) 0 deg C to r.t., 20 min, 2) 40 deg C, 6h;

Reference yield: 93.0%

methanol (67-56-1) + 2,2-Dimethyl-5-(2-phenyltricyclo<3.3.1.13,7>decan-2-yl)-1,3-dioxane-4,6-dione (133709-17-8) → Methyl (2-phenyltricyclo<3.3.1.13,7>decan-2-yl)acetate (133709-20-3)

Guidance literature:

With copper; In pyridine; at 100 ℃; for 9h;

Reference yield: 63.0%

ethanol (64-17-5) + 2,2-Dimethyl-5-(2-phenyltricyclo<3.3.1.13,7>decan-2-yl)-1,3-dioxane-4,6-dione (133709-17-8) → 2-phenyladamantan-2-ol (29480-18-0) + 2-Ethoxy-2-phenyladamantane (133709-19-0)

Guidance literature:

With hydrogenchloride; Yield given. Multistep reaction; 1) reflux, 16h;

upstream raw materials:

2,2-Dimethyl-5-(tricyclo<3.3.1.1^3,7>decanylidene)-1,3-dioxane-4,6-dione

Downstream raw materials:

Methyl (2-phenyltricyclo<3.3.1.1^3,7>decan-2-yl)acetate

2-phenyladamantan-2-ol

2-Ethoxy-2-phenyladamantane

C₁₈H₂₂O₂