Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

Base Information

Chemical Name:Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide
CAS No.:77294-39-4
Molecular Formula:C₁₇H₁₄BrN₃O₃
Molecular Weight:388.22
Hs Code.:

Synonyms:Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

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Chemical Property of Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

Chemical Property:

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Technology Process of Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

There total 3 articles about Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 77294-33-8
6-Bromo-5-hydroxy-2-methyl-1H-indole-3-carboxylic acid hydrazide

: 98-88-4
benzoyl chloride

: 77294-39-4
Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

Guidance literature:: With sodium hydroxide; for 12h; under cooling;

Reference yield:

: 7598-91-6
ethyl 5-hydroxy-2-methylindole-3-carboxylate

: 77294-39-4
Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / acetic acid

2: 85 percent / 80percent N₂H₄*H₂O / ethanol / Heating

3: 86 percent / 10percent aq. NaOH / 12 h / under cooling

With sodium hydroxide; bromine; hydrazine hydrate; In ethanol; acetic acid;

Reference yield:

: 16052-67-8
ethyl 6-bromo-5-hydroxy-2-methyl-indole-3-carboxylate

: 77294-39-4
Benzoic acid N'-(6-bromo-5-hydroxy-2-methyl-1H-indole-3-carbonyl)-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 80percent N₂H₄*H₂O / ethanol / Heating

2: 86 percent / 10percent aq. NaOH / 12 h / under cooling

With sodium hydroxide; hydrazine hydrate; In ethanol;