3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

Base Information

Chemical Name:3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine
CAS No.:98889-57-7
Molecular Formula:C₂₈H₄₃N₃O₉SSi₂
Molecular Weight:653.901
Hs Code.:

Synonyms:3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

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Chemical Property of 3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

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Technology Process of 3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

There total 4 articles about 3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98889-55-5
N³-<(2-nitrophenyl)sulfenyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 74-88-4
methyl iodide

: 98889-57-7
3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

Guidance literature:: With silver(l) oxide; In acetone; at 20 ℃; for 16h;

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 98889-57-7
3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

Guidance literature:: Multi-step reaction with 2 steps

2: 94 percent / Ag₂O / acetone / 16 h / 20 °C

With silver(l) oxide; In acetone;

Reference yield:

: 7669-54-7
2-nitrobenzenesulfenyl chloride

: 98889-57-7
3',5'-O-1,1,3,3-tetraisopropyldisiloxyl-2'-O-methyl-3-N-(2-nitrobenzene)sulfenyluridine

Guidance literature:: Multi-step reaction with 2 steps

2: 94 percent / Ag₂O / acetone / 16 h / 20 °C

With silver(l) oxide; In acetone;