tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Base Information

Chemical Name:tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate
CAS No.:1415217-90-1
Molecular Formula:C₂₈H₄₇NO₅
Molecular Weight:477.685
Hs Code.:

Synonyms:tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

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Technology Process of tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

There total 9 articles about tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: tert-butyl 4-(4-hydroxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

: 77-78-1
dimethyl sulfate

: 1415217-90-1
tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1021/np3007099

Reference yield:

: 219144-65-7
1,2,4,5-tetramethoxy-3-tridecylbenzene

: 1415217-90-1
tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium cerium (IV) nitrate / acetonitrile; water / 3.5 h / -7 - 20 °C / Cooling with ice

2: sodium hydrogencarbonate / ethanol / 27 h / 45 °C / Inert atmosphere

3: potassium carbonate / acetone / Reflux

With ammonium cerium (IV) nitrate; sodium hydrogencarbonate; potassium carbonate; In ethanol; water; acetone; acetonitrile;
DOI:10.1021/np3007099

Reference yield:

: 2441-46-5
1,2,4,5-tetramethoxybenzene

: 1415217-90-1
tert-butyl 4-(4-methoxy-3,6-dioxo-5-tridecylcyclohexa-1,4-dienylamino)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium / tetrahydrofuran; hexane / -40 - 0 °C

1.2: 15 h / 20 °C / Inert atmosphere

2.1: ammonium cerium (IV) nitrate / acetonitrile; water / 3.5 h / -7 - 20 °C / Cooling with ice

3.1: sodium hydrogencarbonate / ethanol / 27 h / 45 °C / Inert atmosphere

4.1: potassium carbonate / acetone / Reflux

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; ammonium cerium (IV) nitrate; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; ethanol; hexane; water; acetone; acetonitrile;
DOI:10.1021/np3007099