N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide

Base Information

• Chemical Name: N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide
• CAS No.: 1232774-52-5
• Molecular Formula: C₁₀H₁₄Cl₃N₂PSe
• Molecular Weight: 378.527

Synonyms:N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide

Chemical Property of N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide

Chemical Property:

Purity/Quality:

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Technology Process of N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide

There total 1 articles about N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonous diamide (1232774-35-4) → N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide (1232774-52-5)

Guidance literature:

With pyridine; selenium; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

Reference yield: 93.0%

N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonoselenoic diamide (1232774-52-5) + dimethyl amine (124-40-3) → 1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide (1232774-71-8)

Guidance literature:

at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.087

upstream raw materials:

N,N-dimethyl-N'-(4-methylphenyl)-P-(trichloromethyl)-phosphonous diamide

Downstream raw materials:

1,1-bis(dimethylamino)-N,N-dimethyl-N'-(4-methylphenyl)-phosphinecarboximidamide selenide

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