5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

Base Information

Chemical Name:5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester
CAS No.:634148-47-3
Molecular Formula:C₂₃H₂₃N₃O₄
Molecular Weight:405.453
Hs Code.:

Synonyms:5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

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Chemical Property of 5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

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Technology Process of 5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

There total 4 articles about 5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 777047-83-3
C₁₃H₁₈N₂O₂

: 15646-46-5
4-ethoxymethylene-2-phenyl-2-oxazolin-5-one

: 634148-47-3
5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

Guidance literature:: In toluene; acetonitrile; at 80 ℃; for 17h;
DOI:10.3987/COM-12-12432

Reference yield: 47.0%

: 331985-92-3
N-(tert-butoxycarbonylmethyl)benzamidine hydrochloride

: 5-oxo-2-phenyl-4,5-dihydro-oxazole-4-carbaldehyde ; sodium-salt

: 634148-47-3
5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

: 1403744-99-9
5-benzoylamino-4-oxo-2-phenyl-1(4H)-pyrimidineacetic acid tert-butyl ester

Guidance literature:: In acetonitrile; at 80 ℃; for 17h;
DOI:10.3987/COM-12-12518

Reference yield:

: 331985-92-3
N-(tert-butoxycarbonylmethyl)benzamidine hydrochloride

: 15646-46-5
4-ethoxymethylene-2-phenyl-2-oxazolin-5-one

: 634148-47-3
5-(benzoylamino)-6-oxo-2-phenyl-1(6H)-pyrimidineacetic acid tert-butyl ester

Guidance literature:: N-(tert-butoxycarbonylmethyl)benzamidine hydrochloride; With sodium carbonate; In water; toluene;

4-ethoxymethylene-2-phenyl-2-oxazolin-5-one; In toluene; acetonitrile; at 20 - 80 ℃;