(3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate

Base Information

Chemical Name:(3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate
CAS No.:1023815-74-8
Molecular Formula:C₂₂H₂₈O₈S₂
Molecular Weight:484.592
Hs Code.:
Mol file:1023815-74-8.mol

Synonyms:(3,3-dimethoxycyclobutane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate)

Suppliers and Price of (3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3,3-Dmethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methylcyclobutyl)methyl4-Methylbenzene-1-sulfonate
100mg
$ 75.00

Synthonix
(3,3-Dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl4-methylbenzene-1-sulfonate 97%
5g
$ 60.00

Synthonix
(3,3-Dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl4-methylbenzene-1-sulfonate 97%
1g
$ 30.00

Total 11 raw suppliers

Chemical Property of (3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

(3,3-Dmethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methylcyclobutyl)methyl4-Methylbenzene-1-sulfonate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate

There total 2 articles about (3,3-dimethoxy-1-{[(4-methylbenzenesulfonyl)oxy]methyl}cyclobutyl)methyl 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 130369-33-4
(1-hydroxymethyl-3,3-dimethoxycyclobutyl)methanol

: 98-59-9
p-toluenesulfonyl chloride

: 1023815-74-8
(3,3-dimethoxycyclobutane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate)

Guidance literature:: With pyridine; at 20 ℃; for 12h; Cooling with ice;

Reference yield:

: 115118-68-8
3,3-dimethoxycyclobutane-1,1-dicarboxylic acid diisopropyl ester

: 1023815-74-8
(3,3-dimethoxycyclobutane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 20 °C

2: pyridine / 12 h / 20 °C / Cooling with ice

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield: 88.0%

: 13195-64-7
diisopropyl malonate

: 1023815-74-8
(3,3-dimethoxycyclobutane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate)

: 1118786-87-0
6,6-dimethoxy-spiro[3.3]heptane-2,2-dicarboxylic acid diisopropyl ester

Guidance literature:: diisopropyl malonate; With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃;

(3,3-dimethoxycyclobutane-1,1-diyl)bis(methylene) bis(4-methylbenzenesulfonate); With potassium iodide; In N,N-dimethyl-formamide; at 120 ℃; for 12h;
DOI:10.1016/j.tetasy.2008.12.016