(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Base Information

Chemical Name:(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester
CAS No.:194222-69-0
Molecular Formula:C₁₂H₈F₆N₂O₁₀S₂
Molecular Weight:518.325
Hs Code.:

Synonyms:(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Suppliers and Price of (2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of (2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

There total 4 articles about (2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78914-94-0
4-methoxyphenyl trifluoromethylsulfide

: 194222-69-0
(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / 35percent aq. H₂O₂ / acetic acid / 48 h / 50 °C

2: 93 percent / 98percent H₂SO₄, HNO₃ / 8 h / 100 °C

3: 1.) pyridine hydrochloride, 2.) POCl₃ / 1.) from 115 deg C to 120 deg C, 2.) reflux, 30 min

4: 1.) t-BuOK / 1.) DMF, 10 min, 2.) DMF, RT, 48 h

With sulfuric acid; potassium tert-butylate; dihydrogen peroxide; nitric acid; pyridine hydrochloride; trichlorophosphate; In acetic acid;
DOI:10.1055/s-1997-1390

Reference yield:

: 15183-74-1
1-methoxy-4-((trifluoromethyl)sulfonyl)benzene

: 194222-69-0
(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 98percent H₂SO₄, HNO₃ / 8 h / 100 °C

2: 1.) pyridine hydrochloride, 2.) POCl₃ / 1.) from 115 deg C to 120 deg C, 2.) reflux, 30 min

3: 1.) t-BuOK / 1.) DMF, 10 min, 2.) DMF, RT, 48 h

With sulfuric acid; potassium tert-butylate; nitric acid; pyridine hydrochloride; trichlorophosphate;
DOI:10.1055/s-1997-1390

Reference yield:

: 19822-29-8
2,6-dinitro-4-((trifluoromethyl)sulfonyl)anisole

: 194222-69-0
(2,6-Dinitro-4-trifluoromethanesulfonyl-phenyl)-trifluoromethanesulfonyl-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine hydrochloride, 2.) POCl₃ / 1.) from 115 deg C to 120 deg C, 2.) reflux, 30 min

2: 1.) t-BuOK / 1.) DMF, 10 min, 2.) DMF, RT, 48 h

With potassium tert-butylate; pyridine hydrochloride; trichlorophosphate;
DOI:10.1055/s-1997-1390