Technology Process of C58H60N2O10S2
There total 4 articles about C58H60N2O10S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-({2-[1,1-bis(4-methoxyphenyl)-1-phenylmethoxy]ethyl}disulfanyl)ethanol; 4-Nitrophenyl chloroformate;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
C32H34N2O5;
With
triethylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 24h;
DOI:10.1002/anie.201311133
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / 3 h / 95 °C
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C
3.2: 24 h / 0 - 20 °C
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201311133
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / 3 h / 95 °C
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C
3.2: 24 h / 0 - 20 °C
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201311133
