C₂₇H₅₁BO₄Si

Base Information

Chemical Name:C₂₇H₅₁BO₄Si
CAS No.:303964-24-1
Molecular Formula:C₂₇H₅₁BO₄Si
Molecular Weight:478.596
Hs Code.:

C<sub>27</sub>H<sub>51</sub>BO<sub>4</sub>Si

Synonyms:C₂₇H₅₁BO₄Si

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Chemical Property of C₂₇H₅₁BO₄Si

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Technology Process of C₂₇H₅₁BO₄Si

There total 10 articles about C₂₇H₅₁BO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116546-78-2
(S)-1-benzyloxy-2-methylpentan-3-one

: 303964-24-1
C₂₇H₅₁BO₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: Et₃N / diethyl ether / 2 h / 0 °C

2.1: diethyl ether / 23 h / -78 - -20 °C

3.1: lithium borohydride / diethyl ether; tetrahydrofuran / 3 h / -78 °C

3.2: 30percent aq. H₂O₂; 10percent aq. NaOH / methanol / 0 - 20 °C

4.1: 99 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -78 °C

5.1: 69 percent / CSA / methanol; CH₂Cl₂ / 8 h / 0 °C

6.1: 100 percent / H₂ / Pd(OH)2/C / ethanol / 16 h / 20 °C

7.1: oxalyl chloride; dimethyl sulfoxide / CH₂Cl₂ / 2 h / -78 - -50 °C

8.1: sodium chlorite; sodium dihydrogen orthophosphate; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 20 °C

9.1: diethyl ether / 20 °C

10.1: Et₃N / diethyl ether / 1 h / 0 °C

With 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; hydrogen; dimethyl sulfoxide; triethylamine; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; tert-butyl alcohol; 7.1: Swern oxidation;
DOI:10.1021/ja011211m

Reference yield:

: 261968-09-6
(2S,3R,4S,5S)-1-benzyloxy-2,4-dimethylhexane-3,5-diol

: 303964-24-1
C₂₇H₅₁BO₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -78 °C

2: 69 percent / CSA / methanol; CH₂Cl₂ / 8 h / 0 °C

3: 100 percent / H₂ / Pd(OH)2/C / ethanol / 16 h / 20 °C

4: oxalyl chloride; dimethyl sulfoxide / CH₂Cl₂ / 2 h / -78 - -50 °C

5: sodium chlorite; sodium dihydrogen orthophosphate; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 20 °C

6: diethyl ether / 20 °C

7: Et₃N / diethyl ether / 1 h / 0 °C

With 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; hydrogen; dimethyl sulfoxide; triethylamine; palladium dihydroxide; In methanol; diethyl ether; ethanol; dichloromethane; water; tert-butyl alcohol; 4: Swern oxidation;
DOI:10.1021/ja011211m

Reference yield:

: 152192-50-2
C₂₅H₃₉BO₂

: 303964-24-1
C₂₇H₅₁BO₄Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: diethyl ether / 23 h / -78 - -20 °C

2.1: lithium borohydride / diethyl ether; tetrahydrofuran / 3 h / -78 °C

2.2: 30percent aq. H₂O₂; 10percent aq. NaOH / methanol / 0 - 20 °C

3.1: 99 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / -78 °C

4.1: 69 percent / CSA / methanol; CH₂Cl₂ / 8 h / 0 °C

5.1: 100 percent / H₂ / Pd(OH)2/C / ethanol / 16 h / 20 °C

6.1: oxalyl chloride; dimethyl sulfoxide / CH₂Cl₂ / 2 h / -78 - -50 °C

7.1: sodium chlorite; sodium dihydrogen orthophosphate; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 20 °C

8.1: diethyl ether / 20 °C

9.1: Et₃N / diethyl ether / 1 h / 0 °C

With 2,6-dimethylpyridine; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; hydrogen; dimethyl sulfoxide; triethylamine; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; tert-butyl alcohol; 6.1: Swern oxidation;
DOI:10.1021/ja011211m