1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol

Base Information

• Chemical Name: 1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol
• CAS No.: 756520-73-7
• Molecular Formula: C19H30 B N O5
• Molecular Weight: 363.262
• Hs Code.: 2934999090
• Mol file: 756520-73-7.mol

Synonyms:1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol;4-(2-Hydroxy-3-(morpholino)propoxy)phenylboronic acid, pinacol ester

Chemical Property of 1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol

Chemical Property:

• Vapor Pressure: 1.19E-11mmHg at 25°C
• Refractive Index: 1.536
• Boiling Point: 520.2°C at 760 mmHg
• Flash Point: 268.4°C
• PSA: 60.39000
• Density: 1.14g/cm³
• LogP: 0.99560

Purity/Quality:

97% ^*data from raw suppliers

4-(2-Hydroxy-3-(morpholino)propoxy)phenylboronicacid,pinacolester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol

There total 2 articles about 1-Morpholino-3-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy)propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

morpholine (110-91-8,99108-56-2) + 4-(oxiran-2-ylmethoxy)phenylboronic acid, pinacol ester (664991-83-7) → 1-morpholin-4-yl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxy]propan-2-ol (756520-73-7)

Guidance literature:

In isopropyl alcohol; at 100 ℃; for 0.5h; Microwave irradiation;

Reference yield:

N-morpholino-3-hydroxyazetidinium chloride (52900-07-9) + 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol (269409-70-3) → 1-morpholin-4-yl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxy]propan-2-ol (756520-73-7)

Guidance literature:

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol; With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 1h;

N-morpholino-3-hydroxyazetidinium chloride; In DMF (N,N-dimethyl-formamide); at 20 ℃;

Reference yield: 43.0%

formic acid (64-18-6) + 1-morpholin-4-yl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxy]propan-2-ol (756520-73-7) + 4-chloro-7-iodo-5-phenyl-5H-pyrrolo[3,2-d]pyrimidine → C25H25ClN4O3*CH2O2

Guidance literature:

1-morpholin-4-yl-3-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenoxy]propan-2-ol; 4-chloro-7-iodo-5-phenyl-5H-pyrrolo[3,2-d]pyrimidine; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In 1,4-dioxane; water; at 120 ℃; Inert atmosphere; Microwave irradiation;

formic acid; In methanol; water;

upstream raw materials:

N-morpholino-3-hydroxyazetidinium chloride

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

morpholine

4-(oxiran-2-ylmethoxy)phenylboronic acid, pinacol ester

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