3,4-dibenzyloxyphenyl boronic acid

Base Information

Chemical Name:3,4-dibenzyloxyphenyl boronic acid
CAS No.:906665-98-3
Molecular Formula:C₂₀H₁₉BO₄
Molecular Weight:334.179
Hs Code.:

Synonyms:3,4-dibenzyloxyphenyl boronic acid

Suppliers and Price of 3,4-dibenzyloxyphenyl boronic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 3,4-dibenzyloxyphenyl boronic acid

Chemical Property:

Boiling Point:536.8±60.0 °C(Predicted)
Density:1.23±0.1 g/cm3(Predicted)

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3,4-dibenzyloxyphenyl boronic acid

There total 2 articles about 3,4-dibenzyloxyphenyl boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 16047-57-7
(((4-bromo-1,2-phenylene)bis(oxy))bis(methylene))dibenzene

: 906665-98-3
3,4-dibenzyloxyphenyl boronic acid

Guidance literature:: (((4-bromo-1,2-phenylene)bis(oxy))bis(methylene))dibenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 4h;

With Triisopropyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2006.05.107

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 16047-57-7
(((4-bromo-1,2-phenylene)bis(oxy))bis(methylene))dibenzene

: 7732-18-5
water

: 906665-98-3
3,4-dibenzyloxyphenyl boronic acid

Guidance literature:: (((4-bromo-1,2-phenylene)bis(oxy))bis(methylene))dibenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 - -60 ℃; for 1h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;

water; With hydrogenchloride; In tetrahydrofuran; hexane; pH=Ca. 1; Cooling;

Reference yield: 100.0%

: 906665-98-3
3,4-dibenzyloxyphenyl boronic acid

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: C₂₅H₂₇BO₄

Guidance literature:: 3,4-dibenzyloxyphenyl boronic acid; 2,2-Dimethyl-1,3-propanediol; In diethyl ether; at 20 ℃; for 14h;

With calcium chloride; In Dimethyl ether; for 1h;
DOI:10.1021/acs.orglett.6b03761