C₂₆H₁₈Cl₃N₃O*ClH

Base Information

Chemical Name:C₂₆H₁₈Cl₃N₃O*ClH
CAS No.:1600565-66-9
Molecular Formula:C₂₆H₁₈Cl₃N₃O*ClH
Molecular Weight:531.268
Hs Code.:

C<sub>26</sub>H<sub>18</sub>Cl<sub>3</sub>N<sub>3</sub>O*ClH

Synonyms:C₂₆H₁₈Cl₃N₃O*ClH

Suppliers and Price of C₂₆H₁₈Cl₃N₃O*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₁₈Cl₃N₃O*ClH

Chemical Property:

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Technology Process of C₂₆H₁₈Cl₃N₃O*ClH

There total 11 articles about C₂₆H₁₈Cl₃N₃O*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1600565-48-7
(4-chlorophenyl)(2,4-dichloro-3-phenylquinolin-6-yl)(1-methyl-1H-imidazol-5-yl)methanol

: 1600565-66-9
C₂₆H₁₈Cl₃N₃O*ClH

: 1600563-25-4
C₂₆H₁₈Cl₃N₃O*ClH

Guidance literature:: (4-chlorophenyl)(2,4-dichloro-3-phenylquinolin-6-yl)(1-methyl-1H-imidazol-5-yl)methanol; In ethanol; Resolution of racemate;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 1600565-66-9
C₂₆H₁₈Cl₃N₃O*ClH

: 1600563-25-4
C₂₆H₁₈Cl₃N₃O*ClH

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 72 h / 20 °C

2.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 0.33 h / Inert atmosphere; Cooling with ice

2.2: 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 1.67 h / 20 °C / Inert atmosphere; Cooling with acetone-dry ice

3.2: Inert atmosphere

4.1: chiral HPLC (Chiralpak AD, 100percent EtOH) / ethanol / Resolution of racemate

With pyridine; n-butyllithium; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;

Reference yield:

: 106-40-1
4-bromo-aniline

: 1600565-66-9
C₂₆H₁₈Cl₃N₃O*ClH

: 1600563-25-4
C₂₆H₁₈Cl₃N₃O*ClH

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 20 h / 90 °C

2.1: n-butyllithium / tetrahydrofuran / 1.67 h / 20 °C / Inert atmosphere; Cooling with acetone-dry ice

2.2: Inert atmosphere

3.1: chiral HPLC (Chiralpak AD, 100percent EtOH) / ethanol / Resolution of racemate

With n-butyllithium; trichlorophosphate; In tetrahydrofuran; ethanol;