2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile

Base Information

• Chemical Name: 2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile
• CAS No.: 71908-64-0
• Molecular Formula: C22H16 N4
• Molecular Weight: 0
• Mol file: 71908-64-0.mol

Synonyms:2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile

Chemical Property of 2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile

Chemical Property:

• PSA: 97.39000
• LogP: 4.51174

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile

There total 3 articles about 2-Amino-6-methyl-4,6-diphenyl-2,4-cyclohexadiene-1,1,3-tricarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-(1-phenylethylidene)propanedinitrile (5447-87-0) → 1-amino-5-methyl-3,5-diphenyl-1,3-cyclohexadiene-2,6,6-tricarbonitrile (71908-64-0)

Guidance literature:

With piperidine; In diethyl ether; for 1.25h; Ambient temperature;

Reference yield: 21.0%

(E)-1-nitrobut-1-ene (27675-37-2) + 2-(1-phenylethylidene)propanedinitrile (5447-87-0) → 2-[3-(nitromethyl)-1-phenylpentylidene]malononitrile (1123797-70-5) + 1-amino-5-methyl-3,5-diphenyl-1,3-cyclohexadiene-2,6,6-tricarbonitrile (71908-64-0)

Guidance literature:

With 1H-imidazole; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1002/ejoc.200800853

Reference yield: 10.0%

2-(1-phenylethylidene)propanedinitrile (5447-87-0) + ethyl 3-oxo-3-phenylpropionate (94-02-0) → 1-amino-5-methyl-3,5-diphenyl-1,3-cyclohexadiene-2,6,6-tricarbonitrile (71908-64-0)

Guidance literature:

With piperidine; In ethanol; for 120h; Ambient temperature;

upstream raw materials:

2-(1-phenylethylidene)propanedinitrile

ethyl 3-oxo-3-phenylpropionate

(E)-1-nitrobut-1-ene

Downstream raw materials:

2-amino-4,6-diphenyl-1,3,5-heptatriene-1,1,3-tricarbonitrile

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