4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Base Information

Chemical Name:4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone
CAS No.:1363807-48-0
Molecular Formula:C₁₈H₂₄N₂OS
Molecular Weight:316.467
Hs Code.:

Synonyms:4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Suppliers and Price of 4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

There total 12 articles about 4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1363807-12-8
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-(1-methylsulfanyl-2-propylidene)hydrazine

: 1363807-48-0
4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 314084-61-2
1-bromo-2,6-diethyl-4-methylbenzene

: 1363807-48-0
4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium; ethylene dibromide / toluene; tetrahydrofuran / 52 h / 40 - 50 °C / Inert atmosphere

1.2: 2 h / 0 - 5 °C / Inert atmosphere

2.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 10 - 20 °C

3.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 2 h / 50 °C / Inert atmosphere

4.1: triethylamine / toluene / 4 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 2.5 h / 0 °C / Inert atmosphere

With thionyl chloride; water; sodium hydride; magnesium; ethylene dibromide; triethylamine; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; toluene;

Reference yield:

: 1363806-98-7
ethyl 2-(2,6-diethyl-4-methylphenyl)-2-oxoacetate

: 1363807-48-0
4-(2,6-diethyl-4-methylphenyl)-2,6-dimethyl-5-methylsulfanyl-2,3-dihydro-3-pyridazinone

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; water / tetrahydrofuran / 3 h / 10 - 20 °C

2: thionyl chloride / N,N-dimethyl-formamide / toluene / 2 h / 50 °C / Inert atmosphere

3: triethylamine / toluene / 4 h / 0 - 20 °C / Inert atmosphere

4: sodium hydride / tetrahydrofuran / 2.5 h / 0 °C / Inert atmosphere

With thionyl chloride; water; sodium hydride; triethylamine; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; toluene;