1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

Base Information

Chemical Name:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine
CAS No.:1363809-07-7
Molecular Formula:C₂₁H₂₄N₂O₂
Molecular Weight:336.434
Hs Code.:

Synonyms:1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

Chemical Property:

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Technology Process of 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

There total 8 articles about 1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1363809-02-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-2-[phenylmethylidene]hydrazine

: 77-78-1
dimethyl sulfate

: 1363809-07-7
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

Guidance literature:: With potassium carbonate; In toluene; at 5 ℃; for 24h;

Reference yield:

: 1363809-02-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-2-[phenylmethylidene]hydrazine

: 77-78-1
dimethyl sulfate

: 1363809-10-2
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

: 1363809-07-7
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 1.5h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 314084-61-2
1-bromo-2,6-diethyl-4-methylbenzene

: 1363809-07-7
1-[2-(2,6-diethyl-4-methylphenyl)-2-oxoacetyl]-1-methyl-2-[phenylmethylidene]hydrazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium; ethylene dibromide / toluene; tetrahydrofuran / 52 h / 40 - 50 °C / Inert atmosphere

1.2: 2 h / 0 - 5 °C / Inert atmosphere

2.1: hydrazine hydrate / methanol / 4.08 h / 1 - 2 °C

3.1: toluene / 2 h / 50 °C / 100 Torr / Inert atmosphere

4.1: potassium carbonate / toluene / 24 h / 5 °C

With potassium carbonate; hydrazine hydrate; magnesium; ethylene dibromide; In tetrahydrofuran; methanol; toluene;