3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone

Base Information

• Chemical Name: 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone
• CAS No.: 119097-12-0
• Molecular Formula: C₁₀H₁₁ClO₄
• Molecular Weight: 230.648

Synonyms:3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone

Chemical Property of 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone

Chemical Property:

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Technology Process of 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone

There total 5 articles about 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

3,5-dichloro-2-dichloromethyl-6-hydroxy-4,4-dimethyl-2,5-cyclohexadienone (119097-07-3) + dimethyl sulfate (77-78-1) → 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-12-0) + 3-chloro-6-formyl-2,5-dimethoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-16-4) + 3-chloro-2,5-dimethoxy-6-dimethoxymethyl-4,4-dimethyl-2,5-cyclohexadienone (119097-11-9)

Guidance literature:

With potassium carbonate; In methanol; at 100 ℃; for 3h; Yield given;

Reference yield: 58.0%

sodium methylate (124-41-4) + 3,5-dichloro-2-dichloromethyl-6-methoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-10-8) → 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-12-0) + 2-formyl-3-hydroxy-5,6-dimethoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-14-2) + 2,3,5-trimethoxy-6-dimethoxymethyl-4,4-dimethyl-2,5-cyclohexadienone (119097-13-1)

Guidance literature:

In methanol; for 1h; Heating;

Reference yield: 20.0%

methanol (67-56-1) + 3,5-dichloro-2-dichloromethyl-6-hydroxy-4,4-dimethyl-2,5-cyclohexadienone (119097-07-3) + dimethyl sulfate (77-78-1) → 3-chloro-6-formyl-5-hydroxy-2-methoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-12-0) + 3,5-dichloro-2-dichloromethyl-6-methoxy-4,4-dimethyl-2,5-cyclohexadienone (119097-10-8) + (E) 3-chloro-6-chloromethylene-2,5,5-trimethoxy-4,4-dimethyl-2-cyclohexenone (119097-22-2) + 3-chloro-2,5-dimethoxy-6-dimethoxymethyl-4,4-dimethyl-2,5-cyclohexadienone (119097-11-9)

Guidance literature:

With potassium carbonate; In dichloromethane; 1.) 20 to 25 deg C, 5 h; 2.) reflux, 28 min;

upstream raw materials:

sodium methylate

3,5-dichloro-2-dichloromethyl-6-methoxy-4,4-dimethyl-2,5-cyclohexadienone

methanol

3,5-dichloro-2-dichloromethyl-6-hydroxy-4,4-dimethyl-2,5-cyclohexadienone

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