[3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine

Base Information

• Chemical Name: [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine
• CAS No.: 291752-74-4
• Molecular Formula: C₃₀H₃₂F₆NOP
• Molecular Weight: 567.554

Synonyms:[3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine

Chemical Property of [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine

Chemical Property:

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Technology Process of [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine

There total 5 articles about [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ⁵-phospha-indan-1-ylidene]-phenyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-triisopropylphenyl lithium (74226-59-8) → [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ5-phospha-indan-1-ylidene]-phenyl-amine (291752-74-4)

Guidance literature:

Multi-step reaction with 3 steps

1: PCl₃ / tetrahydrofuran

3: tetrahydrofuran / -78 °C

With phosphorus trichloride; In tetrahydrofuran; 1: Substitution / 2: Substitution / 3: Substitution;

DOI:10.1016/S0040-4039(00)00829-7

Reference yield:

Phenyl azide (622-37-7) + 3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1-phospha-indan (291752-73-3) → [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ5-phospha-indan-1-ylidene]-phenyl-amine (291752-74-4)

Guidance literature:

In tetrahydrofuran; at -78 ℃;

DOI:10.1016/S0040-4039(00)00829-7

Reference yield:

lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide (70091-67-7) → [3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1λ5-phospha-indan-1-ylidene]-phenyl-amine (291752-74-4)

Guidance literature:

Multi-step reaction with 2 steps

2: tetrahydrofuran / -78 °C

In tetrahydrofuran; 1: Substitution / 2: Substitution;

DOI:10.1016/S0040-4039(00)00829-7

upstream raw materials:

Phenyl azide

3,3-bis-trifluoromethyl-1-(2,4,6-triisopropyl-phenyl)-2-oxa-1-phospha-indan

2,4,6-triisopropyl-1-bromobenzene

lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide

Downstream raw materials:

C₃₃H₃₂F₁₂NO₂P

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