(Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether

Base Information

• Chemical Name: (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether
• CAS No.: 74684-52-9
• Molecular Formula: C₁₈H₁₆F₃NO₄
• Molecular Weight: 367.325

Synonyms:(Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether

Chemical Property of (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether

Chemical Property:

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Technology Process of (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether

There total 4 articles about (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-trifluoroethanol (75-89-8) + (E)-1-Anisyl-2-(p-nitrophenyl)propen-1-yl chloride (74684-45-0) → 1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-1-propanone (74684-47-2) + (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether (74684-52-9) + (E)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether (74684-51-8) + (4-nitrophenyl)ethanone (100-19-6)

Guidance literature:

With 2,6-dimethylpyridine; In water; Rate constant; Product distribution; other bases;

DOI:10.1021/jo01310a011

Reference yield:

2,2,2-trifluoroethanol (75-89-8) + (Z)-1-Anisyl-2-(p-nitrophenyl)propen-1-yl chloride (74684-46-1) → 1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-1-propanone (74684-47-2) + (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether (74684-52-9) + (E)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether (74684-51-8) + (4-nitrophenyl)ethanone (100-19-6)

Guidance literature:

With 2,6-dimethylpyridine; Rate constant; Product distribution; other bases;

DOI:10.1021/jo01310a011

Reference yield:

1-(p-Methoxyphenyl)-1,1,2-trichloro-2-(p-nitrophenyl)-propane (74684-48-3) → (Z)-1-(p-Methoxyphenyl)-2-(p-nitrophenyl)-propen-1-yl trifluoroethyl ether (74684-52-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium iodide / acetone / Heating

2: various solvent(s) / 48 h / 120 °C

With sodium iodide; In acetone;

DOI:10.1021/jo01310a011

upstream raw materials:

2,2,2-trifluoroethanol

(E)-1-Anisyl-2-(p-nitrophenyl)propen-1-yl chloride

(Z)-1-Anisyl-2-(p-nitrophenyl)propen-1-yl chloride

sodium 2,2,2-trifluoroethanolate

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