benzylmethyl phenylphosphonate

Base Information

Chemical Name:benzylmethyl phenylphosphonate
CAS No.:146849-38-9
Molecular Formula:C₁₄H₁₅O₃P
Molecular Weight:262.245
Hs Code.:

Synonyms:benzylmethyl phenylphosphonate

Suppliers and Price of benzylmethyl phenylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of benzylmethyl phenylphosphonate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of benzylmethyl phenylphosphonate

There total 2 articles about benzylmethyl phenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 67-56-1
methanol

: 100-51-6,185532-71-2
benzyl alcohol

: 146849-38-9
benzylmethyl phenylphosphonate

Guidance literature:: P,P-dichlorophenylphosphine oxide; benzyl alcohol; With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; In benzene; at 0 - 20 ℃; for 3h;

methanol; With N-ethyl-N,N-diisopropylamine; In benzene; for 3h; Further stages.;
DOI:10.1016/j.tetlet.2004.06.083

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 67-56-1
methanol

: 100-51-6,185532-71-2
benzyl alcohol

: 19236-61-4
dibenzyl phenylphosphonate

: 146849-38-9
benzylmethyl phenylphosphonate

: 2240-41-7
dimethyl phenylphosphonate

Guidance literature:: With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction. Yields of byproduct given; 1) benzene, r.t., overnight, 2) 10 min;
DOI:10.1016/S0040-4020(01)80305-7

Reference yield: 82.0%

: 146849-38-9
benzylmethyl phenylphosphonate

: 10088-45-6
methyl phenylphosphonic acid

Guidance literature:: With trifluorormethanesulfonic acid; In toluene; at 120 ℃; for 24h; Sealed tube; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.0c00550