4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

Base Information

Chemical Name:4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester
CAS No.:1332699-73-6
Molecular Formula:C₃₉H₄₂N₂O₇S₃
Molecular Weight:746.97
Hs Code.:

4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

Synonyms:4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

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Chemical Property of 4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

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Technology Process of 4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

There total 10 articles about 4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332699-66-7
2-amino-4-benzenesulfinyl-2-(2-benzenesulfinylethyl)butyric acid methyl ester

: C₂₀H₁₉NO₄S

: 1332699-73-6
4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

Guidance literature:: With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol201980r

Reference yield:

: 1332699-70-3
3-[2-(tert-butyldiphenylsilanyloxy)ethyl]-5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indole

: 1332699-73-6
4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/ol201980r

Reference yield:

: 1332699-71-4
2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethanol

: 1332699-73-6
4-benzenesulfinyl-2-(2-benzenesulfinylethyl)-2-{2-[5-methoxy-1-(toluene-4-sulfonyl)-2-vinyl-1H-indol-3-yl]ethylamino}butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 3 h / 80 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / dichloromethane / 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; ethyl acetate;
DOI:10.1021/ol201980r