IMes*CSNPh

Base Information

Chemical Name:IMes*CSNPh
CAS No.:1312029-25-6
Molecular Formula:C₂₈H₂₉N₃S
Molecular Weight:439.624
Hs Code.:

Synonyms:IMes*CSNPh

Suppliers and Price of IMes*CSNPh

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of IMes*CSNPh

Chemical Property:

Purity/Quality:

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Technology Process of IMes*CSNPh

There total 2 articles about IMes*CSNPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 103-72-0
phenyl isothiocyanate

: 141556-42-5
[1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene

: 1312029-25-6
IMes*CSNPh

Guidance literature:: In tetrahydrofuran; at 20 ℃; Temperature; Solvent; Kinetics; Equilibrium constant; Inert atmosphere;
DOI:10.1021/jo101850g

Reference yield: 81.0%

: 103-72-0
phenyl isothiocyanate

: 141556-45-8
1,3-bis(mesityl)imidazolium chloride

: 1312029-25-6
IMes*CSNPh

Guidance literature:: With sodium hydride; In tetrahydrofuran; mineral oil; at 10 - 15 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c0dt01613f

Reference yield: 74.0%

: 37095-27-5
(bis(diphenylphosphino)methane)bis(chlorogold(I))

: 1312029-25-6
IMes*CSNPh

: 2923-28-6
silver trifluoromethanesulfonate

: [(bis(diphenylphosphino)methane)Au₂(SCNPh*IMes)](OTf)2

Guidance literature:: In tetrahydrofuran; (N2) to soln. Au complex in THF was treated with soln. AgOTf in THF, stirred for 45 min at 0°C in the dark, soln. was filtered and added to soln. ligand in THF, stirred for 2 h at 0°C; solvents were removed in vacuo, residue was dissolved in CH2Cl2, filtered through Celite, pentane was added;
DOI:10.1039/c0dt01613f