5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

Base Information

Chemical Name:5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide
CAS No.:1350324-79-6
Molecular Formula:C₈₀H₁₀₄N₅O₃*I
Molecular Weight:1310.64
Hs Code.:

Synonyms:5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

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Chemical Property of 5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

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Technology Process of 5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

There total 3 articles about 5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5-(4-pyridyl)-10,15,20-tris(4-dodecyloxyphenyl)-porphyrin

: 74-88-4
methyl iodide

: 1350324-79-6
5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

Guidance literature:: In chloroform; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1142/S1088424611003471

Reference yield:

: 143-15-7
1-dodecylbromide

: 1350324-79-6
5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 16 h / 70 °C

2: oxygen; propionic acid / 2.5 h / Reflux; Darkness

3: chloroform; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With oxygen; potassium carbonate; propionic acid; potassium iodide; In chloroform; N,N-dimethyl-formamide;
DOI:10.1142/S1088424611003471

Reference yield:

: 24083-19-0
4-n-dodecyloxybenzaldehyde

: 52073-75-3
meso-(4-pyridyl)-2,2'-dipyrromethane

: 1350324-79-6
5-(N-methylpyridinium-4-yl)-10,15,20-tris(4-dodecyloxyphenyl)porphyrin iodide

Guidance literature:: Multi-step reaction with 2 steps

1: oxygen; propionic acid / 2.5 h / Reflux; Darkness

2: chloroform; N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With oxygen; propionic acid; In chloroform; N,N-dimethyl-formamide;
DOI:10.1142/S1088424611003471