phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:85372-99-2
Molecular Formula:C₃₂H₄₀O₁₈
Molecular Weight:712.659
Hs Code.:

Synonyms:phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

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Chemical Property of phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

There total 3 articles about phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 22352-62-1
O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

: 108-95-2,27073-41-2
phenol

: 85372-99-2
phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With zinc(II) chloride; at 100 ℃; for 2h;
DOI:10.1016/0008-6215(83)88243-3

Reference yield:

: 85439-68-5
2,4,6-tri-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranosyl bromide

: 85372-99-2
phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / acetic acid / 4 h / Ambient temperature

2: 60 percent / zinc chloride / 2 h / 100 °C

With zinc(II) chloride; In acetic acid;
DOI:10.1016/0008-6215(83)88243-3

Reference yield:

: 68036-16-8
1,2,4,6-tetra-O-acetyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranose

: 85372-99-2
phenyl 2,4-di-O-acteyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / hydrogen bromide / acetic acid / 1 h / Ambient temperature

2: 92 percent / acetic acid / 4 h / Ambient temperature

3: 60 percent / zinc chloride / 2 h / 100 °C

With hydrogen bromide; zinc(II) chloride; In acetic acid;
DOI:10.1016/0008-6215(83)88243-3