C₃₂H₃₂O₇

Base Information

Chemical Name:C₃₂H₃₂O₇
CAS No.:1365537-14-9
Molecular Formula:C₃₂H₃₂O₇
Molecular Weight:528.602
Hs Code.:

C<sub>32</sub>H<sub>32</sub>O<sub>7</sub>

Synonyms:C₃₂H₃₂O₇

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Chemical Property of C₃₂H₃₂O₇

Chemical Property:

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Technology Process of C₃₂H₃₂O₇

There total 16 articles about C₃₂H₃₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1365537-11-6
C₃₂H₃₀O₇

: 1365537-14-9
C₃₂H₃₂O₇

Guidance literature:: With aluminum isopropoxide; isopropyl alcohol; In toluene; at 100 ℃; for 1h;
DOI:10.1016/j.tetlet.2012.01.054

Reference yield:

: 1365536-83-9
1-(2-(benzyloxy)-6-hydroxy-4-(methoxymethoxy)phenyl)ethan-1-one

: 1365537-14-9
C₃₂H₃₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

1.2: 1.08 h / 0 - 20 °C

1.3: 0 °C

2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; ethanol / 5.08 h / -40 - 0 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C

4.1: AD-mix-α; methanesulfonamide; water / tetrahydrofuran; tert-butyl alcohol / 16 h / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C

6.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C

7.1: methanol; ammonia / 48 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane; water / 2 h

9.1: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / 100 °C

With 1H-imidazole; methanol; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; ammonia; water; pyridinium p-toluenesulfonate; aluminum isopropoxide; sodium hydride; Dess-Martin periodane; acetic acid; isopropyl alcohol; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; mineral oil; tert-butyl alcohol; 4.1: Sharpless dihydroxylation / 9.1: Meerwein-Ponndorf-Verley reduction;
DOI:10.1016/j.tetlet.2012.01.054

Reference yield:

: 1365537-00-3
C₃₈H₄₈O₈Si

: 1365537-14-9
C₃₂H₃₂O₇

Guidance literature:: Multi-step reaction with 5 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C

2: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C

3: methanol; ammonia / 48 h / 20 °C

4: Dess-Martin periodane / dichloromethane; water / 2 h

5: aluminum isopropoxide; isopropyl alcohol / toluene / 1 h / 100 °C

With methanol; tetrabutyl ammonium fluoride; ammonia; pyridinium p-toluenesulfonate; aluminum isopropoxide; Dess-Martin periodane; acetic acid; isopropyl alcohol; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; toluene; 5: Meerwein-Ponndorf-Verley reduction;
DOI:10.1016/j.tetlet.2012.01.054