methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

Base Information

Chemical Name:methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside
CAS No.:1242144-28-0
Molecular Formula:C₂₀H₃₄O₅Si
Molecular Weight:382.572
Hs Code.:

Synonyms:methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

Suppliers and Price of methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

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Technology Process of methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

There total 1 articles about methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1242144-26-8
methyl 5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

: 100-39-0
benzyl bromide

: 1242144-28-0
methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; oil; at 0 - 20 ℃;
DOI:10.1016/j.carres.2010.05.003

Reference yield: 91.0%

: 1242144-28-0
methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

: 108-24-7
acetic anhydride

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1353040-49-9
(2S,3R,4R)-3-benzyloxy-1,2-di-tertbutyldimethylsilyloxy-4-methoxyoctadec-5-ene

Guidance literature:: methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside; acetic anhydride; With sulfuric acid; at 20 ℃; for 1h;

With potassium hydroxide; In methanol; at 20 ℃; for 16h;

n-tridecyltriphenylphosphonium bromide; tert-butyldimethylsilyl chloride; Further stages;
DOI:10.1016/j.carres.2010.05.003

Reference yield: 75.0%

: 1242144-28-0
methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside

: 108-24-7
acetic anhydride

: 18162-48-6
tert-butyldimethylsilyl chloride

: 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-L-ribofuranose

: 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-L-ribopyranose

Guidance literature:: methyl 3-O-benzyl-5-O-tert-butyldimethylsilyl-2-O-methyl-β-L-ribofuranoside; acetic anhydride; With sulfuric acid; at 20 ℃; for 1h;

With potassium hydroxide; In methanol; at 20 ℃; for 16h;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In dichloromethane; at 20 ℃; for 0.75h;
DOI:10.1016/j.carres.2010.05.003