(-)-(R)-3-methoxytyrosine methyl ester hydrochloride

Base Information

Chemical Name:(-)-(R)-3-methoxytyrosine methyl ester hydrochloride
CAS No.:113948-38-2
Molecular Formula:C₁₁H₁₅NO₄*ClH
Molecular Weight:261.705
Hs Code.:

Synonyms:(-)-(R)-3-methoxytyrosine methyl ester hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(R)-3-methoxytyrosine methyl ester hydrochloride

Chemical Property:

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Technology Process of (-)-(R)-3-methoxytyrosine methyl ester hydrochloride

There total 3 articles about (-)-(R)-3-methoxytyrosine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 15402-76-3,4214-13-5
(+)-(R)-3-methoxytyrosine

: 113948-38-2
(-)-(R)-3-methoxytyrosine methyl ester hydrochloride

Guidance literature:: With thionyl chloride; at -10 ℃; for 0.75h;
DOI:10.1021/jo00245a035

Reference yield:

: 55739-56-5
α-acetamido-3-methoxy-4-acetoxycinnamic acid

: 113948-38-2
(-)-(R)-3-methoxytyrosine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / (μ-dichloro)tetraethylenedirhodium(I), (-)-2,3-O-isopropylidene-2,3-dihydroxy-1,4-bis(diphenylphosphino)butane, H2 / ethanol; benzene / 12 h

2: 100 percent / 20percent aq. H₂SO₄ / 4 h / Heating

3: 100 percent / thionyl chloride / 0.75 h / -10 °C

With thionyl chloride; bis(ethylene)rhodium(I) chloride dimer; sulfuric acid; hydrogen; (-)-2,3-O-isopropylidene-2,3-dihydroxy-1,4-bis(diphenylphosphanyl)butane; In ethanol; benzene;
DOI:10.1021/jo00245a035

Reference yield:

: 30948-27-7
(R)-N-acetyl-3-(4-acetoxy-3-methoxyphenyl)alanine

: 113948-38-2
(-)-(R)-3-methoxytyrosine methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 20percent aq. H₂SO₄ / 4 h / Heating

2: 100 percent / thionyl chloride / 0.75 h / -10 °C

With thionyl chloride; sulfuric acid;
DOI:10.1021/jo00245a035