N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

Base Information

Chemical Name:N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide
CAS No.:1357161-90-0
Molecular Formula:C₁₈H₁₂BrCl₃F₃N₃O₂
Molecular Weight:545.57
Hs Code.:

Synonyms:N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

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Chemical Property of N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

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Technology Process of N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

There total 7 articles about N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tert-butyl N'-(2-bromoethyl)-N-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbazate

: 1357161-90-0
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.5h;

Reference yield:

: 1237587-86-8
tert-butyl {2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}carbamate

: 1357161-90-0
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C

1.2: 0.25 h / 20 °C

2.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

3.1: trifluoroacetic acid / 0.5 h / 20 °C

With sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; mineral oil;

Reference yield:

: 66399-01-7
2-chloro-5-hydroxyiminomethylnitrobenzene

: 1357161-90-0
N'-{2-chloro-5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}-2-bromoacetohydrazide

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 0.83 h / 75 °C

3.1: bis(trichloromethyl) carbonate / toluene; tetrahydrofuran / 1 h / 20 - 80 °C

3.2: 16 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 20 °C

4.2: 0.25 h / 20 °C

5.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

6.1: trifluoroacetic acid / 0.5 h / 20 °C

With N-chloro-succinimide; bis(trichloromethyl) carbonate; water; iron; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; toluene; mineral oil;