(Z)-β-(cyclohexylmethyl)styrene

Base Information

Chemical Name:(Z)-β-(cyclohexylmethyl)styrene
CAS No.:1454834-24-2
Molecular Formula:C₁₅H₂₀
Molecular Weight:200.324
Hs Code.:

Synonyms:(Z)-β-(cyclohexylmethyl)styrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-β-(cyclohexylmethyl)styrene

Chemical Property:

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Technology Process of (Z)-β-(cyclohexylmethyl)styrene

There total 5 articles about (Z)-β-(cyclohexylmethyl)styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5044-52-0
vinyltriphenylphosphonium bromide

: 100-52-7
benzaldehyde

: 98-89-5
Cyclohexanecarboxylic acid

: 1454834-24-2
(Z)-β-(cyclohexylmethyl)styrene

: (E)-(3-cyclohexylprop-1-en-1-yl)benzene

Guidance literature:: vinyltriphenylphosphonium bromide; Cyclohexanecarboxylic acid; With potassium phosphate; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique; Sealed tube; Irradiation;

benzaldehyde; In tetrahydrofuran; at 60 ℃; for 16h; Overall yield = 52 percent; stereoselective reaction; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1038/s41557-021-00807-x

Reference yield:

: 87802-71-9,85217-69-2
(E)-methyl cinnamyl carbonate

: 1539-59-9
4-cyclohexyl-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester

: 1454834-24-2
(Z)-β-(cyclohexylmethyl)styrene

: (E)-(3-cyclohexylprop-1-en-1-yl)benzene

Guidance literature:: With DMP*NiCl₂; 2,4,5,6-tetrakis(carbazol-9-yl)-4,6-dicyanobenzene; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Reagent/catalyst; regioselective reaction; Sealed tube; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.9b02473

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: C₁₆H₃₆O₂Si₃

: 1454834-24-2
(Z)-β-(cyclohexylmethyl)styrene

: (E)-(3-cyclohexylprop-1-en-1-yl)benzene

Guidance literature:: With potassium trimethylsilonate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; In tetrahydrofuran; at 50 ℃; for 15h; Overall yield = 119 mg;
DOI:10.1002/anie.201304084