1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Base Information

Chemical Name:1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether
CAS No.:131610-00-9
Molecular Formula:C₁₉H₂₉NO₂SSi
Molecular Weight:363.596
Hs Code.:

Synonyms:1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Suppliers and Price of 1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

There total 4 articles about 1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 131610-00-9
1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide / 18 h / Ambient temperature

2: 1.) n-BuLi / 1.) ether, hexane, -70 deg C, 2.) ether, hexane, from -70 deg C to RT

3: 1.) NaH / 1.) THF, 2.) THF, RT, 2 h

With 1H-imidazole; n-butyllithium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm00111a038

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 131610-00-9
1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide / 18 h / Ambient temperature

2: 1.) n-BuLi / 1.) ether, hexane, -70 deg C, 2.) ether, hexane, from -70 deg C to RT

3: 1.) NaH / 1.) THF, 2.) THF, RT, 2 h

With 1H-imidazole; n-butyllithium; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1021/jm00111a038

Reference yield:

: 134154-50-0
3-(tert-butyldimethylsilyloxy)phenyl ethyl ketone

: 131610-00-9
1-<3-<(tert-butyldimethylsilyl)oxy>phenyl>-1-(thiazol-2-yl)propyl methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) ether, hexane, -70 deg C, 2.) ether, hexane, from -70 deg C to RT

2: 1.) NaH / 1.) THF, 2.) THF, RT, 2 h

With n-butyllithium; sodium hydride;
DOI:10.1021/jm00111a038