(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

Base Information

Chemical Name:(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)
CAS No.:219603-31-3
Molecular Formula:C₃₀H₂₅NO₈
Molecular Weight:527.53
Hs Code.:

Synonyms:(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

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Chemical Property of (1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

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Technology Process of (1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

There total 8 articles about (1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 219603-30-2
(1R,2S)-(2-(4-((tert-butyldimethylsilyl)oxy)benzamido)-1-phenyl-1,3-propanediyl)bis(4-((tert-butyldimethylsilyl)oxy)benzoate)

: 219603-31-3
(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1021/jo981508b

Reference yield: 52.0%

: 219603-32-4
(1R,2S)-(2-(4-(benzyloxy)benzamido)-1-phenyl-1,3-propanediyl)bis(4-(benzyloxy)benzoate)

: 219603-31-3
(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

Guidance literature:: With hydrogen; W-2 Raney Ni; In methanol; ethyl acetate; for 18h; under 760 Torr;
DOI:10.1021/jo981508b

Reference yield:

: 1486-50-6
4-(benzyloxy)benzoic acid chloride

: 219603-31-3
(1R,2S)-(2-(4-hydroxybenzamido)-1-phenyl-1,3-propanediyl)bis(4-hydoxybenzoate)

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / 4-dimethylaminopyridine; pyridine

2: 52 percent / H₂ / Raney Ni / methanol; ethyl acetate

With pyridine; dmap; hydrogen; nickel; In methanol; ethyl acetate;
DOI:10.1021/jo010423z