(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

Base Information

Chemical Name:(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol
CAS No.:1454866-41-1
Molecular Formula:C₂₁H₂₆Cl₂N₂O
Molecular Weight:393.356
Hs Code.:

Synonyms:(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

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Chemical Property of (S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

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Technology Process of (S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

There total 6 articles about (S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 22795-99-9
(S)-2-(Aminomethyl)-1-ethylpyrrolidine

: 100-52-7
benzaldehyde

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 1454866-41-1
(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

Guidance literature:: (S)-2-(Aminomethyl)-1-ethylpyrrolidine; benzaldehyde; In ethanol; for 24h; Reflux;

With sodium tetrahydroborate; In ethanol; for 3h;

formaldehyd; 2,4-dichlorophenol; In ethanol; for 12h; Reflux;

Reference yield: 59.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1454866-36-4
(S)-N-benzyl-1-(1-ethylpyrrolidin-2-yl)methanamine

: 120-83-2,40477-79-0
2,4-dichlorophenol

: 1454866-41-1
(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

Guidance literature:: In ethanol; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c3cc44980g

Reference yield:

: C₁₄H₂₀N₂

: 1454866-41-1
(S)-2-{N-benzyl-N-[(1-ethylpyrrolidin-2-yl)methyl]aminomethyl}-4,6-dichlorophenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 3 h / 60 °C / Inert atmosphere

2: ethanol / 12 h / 90 °C / Inert atmosphere

With sodium tetrahydroborate; In ethanol;
DOI:10.1039/c3cc44980g