Technology Process of olivetol carboxylic acid dimethyl ether
There total 16 articles about olivetol carboxylic acid dimethyl ether which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium;
Yield given. Multistep reaction;
1.) ether, 2 h;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 78 percent / hydrazine hydrate / 2 h / Heating
2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C
3: 93 percent / toluene / 2.5 h / Heating
4: 8.7 g / sodium hydroxide (20percent) / 60 °C
8: 28.8 g / fluoroboric acid, sodium nitrite / H2O
9: 7.6 g / warming, distillation
10: 1.) lithium / 1.) ether, 2 h
With
hydrogenchloride; sodium hydroxide; tetrafluoroboric acid; lithium; hydrazine hydrate; acetic acid; sodium nitrite;
In
water; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 84 percent / sodium hydroxide / heating
5: 28.8 g / fluoroboric acid, sodium nitrite / H2O
6: 7.6 g / warming, distillation
7: 1.) lithium / 1.) ether, 2 h
With
sodium hydroxide; tetrafluoroboric acid; lithium; sodium nitrite;
In
water;
