4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

Base Information

Chemical Name:4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol
CAS No.:154694-14-1
Molecular Formula:C₁₇H₁₄BrN₃O₂S
Molecular Weight:404.287
Hs Code.:

Synonyms:4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

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Technology Process of 4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

There total 3 articles about 4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5351-92-8
vanillin thiosemicarbazone

: 99-90-1
para-bromoacetophenone

: 154694-14-1
4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

Guidance literature:: In ethanol; at 100 ℃;
DOI:10.1016/j.bioorg.2020.104088

Reference yield: 72.0%

: 5351-92-8
vanillin thiosemicarbazone

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 154694-14-1
4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

Guidance literature:: In ethanol; Reflux;
DOI:10.1248/cpb.c14-00616

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 154694-14-1
4-({2-[4-(4-bromophenyl)-1,3-thiazol-2-yl]hydrazinylidene}-methyl)-2-methoxyphenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / ethanol / 0.5 h

1.2: 2 h / 100 °C

2.1: ethanol / 100 °C

With sulfuric acid; In ethanol;
DOI:10.1016/j.bioorg.2020.104088