4-IODODIPHENYL ETHER

Base Information

• Chemical Name: 4-IODODIPHENYL ETHER
• CAS No.: 2974-94-9
• Molecular Formula: C12H9IO
• Molecular Weight: 296.107
• Hs Code.: 2909309090
• Mol file: 2974-94-9.mol

Synonyms:Ether,p-iodophenyl phenyl (6CI,7CI,8CI);1-Iodo-4-phenoxybenzene;4-Iododiphenylether;4-Iodophenyl phenyl ether;4-Phenoxyiodobenzene;Phenyl iodophenylether;p-Phenoxyiodobenzene;

Chemical Property of 4-IODODIPHENYL ETHER

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 43～45℃
• Refractive Index: 1.65
• Boiling Point: 317.6 °C at 760 mmHg
• Flash Point: 145.9 °C
• PSA: 9.23000
• Density: 1.626 g/cm³
• LogP: 4.08350
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

1-Iodo-4-phenoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-IODODIPHENYL ETHER

There total 18 articles about 4-IODODIPHENYL ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diphenylether (101-84-8) → 4-phenoxyiodobenzene (2974-94-9)

Guidance literature:

With N-iodo-succinimide; iron(III) chloride; In acetonitrile; at 25 ℃; for 0.5h;

DOI:10.1246/cl.2003.932

Reference yield: 95.0%

p-Iodophenol (540-38-5) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 4-phenoxyiodobenzene (2974-94-9)

Guidance literature:

With cesium fluoride; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1021/ol0361406

Reference yield: 87.0%

p-Iodophenol (540-38-5) + Diphenyliodonium triflate (66003-76-7) → 4-phenoxyiodobenzene (2974-94-9)

Guidance literature:

p-Iodophenol; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.25h;

Diphenyliodonium triflate; In tetrahydrofuran; at 40 ℃; for 0.5h;

DOI:10.1021/ol200265t

upstream raw materials:

diphenylether

4-phenoxyanilin

para-iodoanisole

benzenediazonium tetrafluoroborate

Downstream raw materials:

4-Phenoxybenzoic acid

5-iodo-2-phenoxy-benzoic acid

bis(4-iodophenyl) ether

1-(4-nitrophenoxy)-4-iodobenzene

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