C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

Base Information

Chemical Name:C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2
CAS No.:882866-11-7
Molecular Formula:C₂₀H₂₃NO₂
Molecular Weight:309.408
Hs Code.:

C<sub>6</sub>H<sub>3</sub>OCH<sub>2</sub>OCHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2

Synonyms:C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

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Chemical Property of C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

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Technology Process of C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

There total 1 articles about C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6852-54-6
N-(benzylidene)ethylamine

: 130517-95-2,54089-45-1
piperonal N-benzylimine

: 882866-11-7
C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

: 780-25-6
N-benzylidene benzylamine

: 117696-79-4
N-(2,6-diisopropylphenyl)-1-phenylmethanimine

: 80985-00-8
3,4-methylenedioxybenzylideneethylamine

Guidance literature:: In toluene; at 80 ℃; for 50h; Catalytic behavior; Schlenk technique; Glovebox;
DOI:10.1021/acs.organomet.7b00115

Reference yield: 83.0%

: 7681-65-4
copper(l) iodide

: 882866-11-7
C₆H₃OCH₂OCHNC₆H₃(CH(CH₃)2)2

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1354550-47-2
(CuI(C₆H₅)2PC₆H₂OCH₂OCHNC₆H₃(CH(CH₃)2)2)2

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; toluene; byproducts: LiCl; (N2); addn. of toluene to ligand, addn. of a soln. of Li compd. in hexane, stirring for 30 min, addn. to a slurry of CuI in Et2O, stirring for 30 min, addn. of phosphine, stirring for 20 min; evapn. in vac., dissolving in CH2Cl2, filtration through celite, washingwith CH2Cl2, evapn. in vac., washing with pentane, drying in vac.;
DOI:10.1039/c1dt11629k